Morphological and Structural Characteristics of the Iron Fluoride Preparated by Solvotermal Synthesis

Array

Authors

  • V.V. Moklyak Institute of Metal Physics. G.V. Kurdyumov NAS of Ukraine
  • V.О. Kotsyubynsky Vasyl Stefanyk Prekarpathian University
  • A.B. Hrubiak Vasyl Stefanyk Prekarpathian University
  • L.Z. Zbihlei Institute of Metal Physics, National Academy of Science

DOI:

https://doi.org/10.15330/pcss.17.3.356-362

Keywords:

iron fluoride, nanoparticles, solvotermal synthesis, crystal structure, dehydration, Mössbauer spectroscopy

Abstract

In this communication we demonstrate the fast and facile preparation of nanoparticles hydrated and anhydrous iron trifluoride by solvotermal synthesis using the surface active substances. The iron fluoride/acytelen black composites were prepared by ultrasonic treatment. The analysis of the crystal microstructure and morphological properties of the material received.

References

[1] T. Li, L. Li, Y.L. Cao, X.P. Ai, H.X. Yang, J. Phys. Chem. 114, 3190 (2010).
[2] Li Liu, Haipeng Guo, Meng Zhou, Qiliang Wei, Zhenhua Yang, Hongbo Shu, Xiukang Yang, Jinli Tan, Zichao Yan, Xianyou Wang, Journal of Power Sources 238, 501 (2013).
[3] L. Liu, M. Zhou, L.H. Yi, H.P. Guo, J.L. Tan, H.B. Shu, X.K. Yang, Z.H. Yang, X.Y. Wang, J. Mater. Chem. 22, 17539 (2012).
[4] F. Badway, N. Pereira, F. Cosandey, G.G. Amatucci, Journal of the Electrochemical Society 150, A1209 (2003).
[5] J. Wang, X. Sun, Energy & Environmental Science 5, 5163 (2012).
[6] M. C. Morris, F. H. McMurdie, H. Eloise, B. Paretzkin, Standart X-ray Diffraction Powder Patterns (Nat. Bur. Stand Washington, D.C.: Monogr 25-Sec 17. 1980), p. 114.
[7] V.V. Moklyak, V.O. Kotsyubyns'kyy, P.I. Kolkovs'kyy, A.B. Hrub"yak, L.Z. Zbihley, Metallofyzyka y noveyshye tekhnolohyy 37 (3), 355 (2015).
[8] G. Teufer, Acta Cryst., (Engineering Materials Laboratory, Engineering Department, E.I. du Pont de Nemours & Co., Inc., Wilmington, Delaware, U.S.A.)(Thessis Received 19 May 1964): p. 1480.
[9] MC Morris, HF McMurdie, EH Evans et al., X-ray diffraction powder patterns, (National bureau of standards, Washington, 1981).
[10] Tan J., Liu L., Hu H., Yang Z., Guo H., Wei Q., Shu H, J POWER SOURCES. 251, 75 (2014).

Published

2016-09-15

How to Cite

Moklyak, V., Kotsyubynsky, V., Hrubiak, A., & Zbihlei, L. (2016). Morphological and Structural Characteristics of the Iron Fluoride Preparated by Solvotermal Synthesis: Array. Physics and Chemistry of Solid State, 17(3), 356–362. https://doi.org/10.15330/pcss.17.3.356-362

Issue

Section

Scientific articles

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